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Characterization Instruments

Instrument Name -> Talos F200X Helios Nanolab HeliScan Mk2 Quanta 250 K-Alpha Xeuss 2.0 Equinox 100
Instrument Type -> TEM FIB-SEM MicroCT E-SEM XPS SAXS XRD
1W or LaB6 
Academic & Non-Profit (independent) $78 $75 $20 $48 $48 $27 $30
Academic & Non-Profit (assisted) $153 $150 $95 $113 $113 $92 $95
Academic & Non-Profit (after hours/auto2,3) $52 $50 $20 $32 $32 $18 $30
For-profit business (independent) $270 $260 $210 $160 $180 $60 $50
For-profit business (assisted) $390 $380 $330 $280 $300 $180 $170
For-profit business (automated) $104 $100 $100 $64 $85 $25 $50

Make sure to read note 3 at the bottom of the page to learn about automated sessions! Charges are capped for automated overnight and weekend sessions! Ask EMC staff members for more details.

 

Sample Preparation Equipment (Physical Sciences)

Instrument Name -> IB-19520CCP Prep' Eqpt Type A4 Prep' Eqpt Type B4
Instrument Type -> cross-section polisher sample preparation carbon/sputter coater
Academic & Non-Profit (unassisted) $20 $30 $15
Academic & Non-Profit (assisted) $85 $30 + staff time $15 + staff time
Academic & Non-Profit (after hours/auto2,3) $20 n/a n/a
For-profit business (unassisted) $50 $60 $30
For-profit business (assisted) $170 $60 + staff time $30 + staff time
For-profit business (automated) $50 n/a n/a

Staff Assistance

 

University

of Kentucky

External Academic

& Non-Profit

External For-Profit
EMC staff labor/hr (sample preparation, data analysis, reports, etc.) $65 $90 $120

Life Sciences Sample Preparation

Service -> TEM sample preparation package TEM sample preparation package TEM sample preparation training Additional staff assistance (Life Sciences sample preparation)
  1 to 4 samples 5 to 10 samples in addition to TEM sample preparation fee per hour
University of Kentucky (independent) n/a n/a n/a n/a
University of Kentucky (assisted) $1,800 $2,500 $700 $100
External academic & Non-profit (independent) n/a n/a n/a n/a
External academic & Non-profit (assisted) $2,200 $2,900 $1,000 $150
External For-profit (independent) n/a n/a n/a n/a
External For-profit (assisted) $3,500 $4,800 n/a $200

The TEM sample preparation packages include all preparation steps (fixation-staining-embedding-sectioning), supplies and chemicals.

For more information regarding training, please contact Dr. Jian Pu.

Life Sciences Sample Preparation (Cont'd)

Service ->SectioningStaining & ImmunolabellingResin EmbeddingIndependent lab use (no chemicals supplied)Independent lab use (chemicals supplied)
 per hourper hourset of 5 to 10 samplesper hourper hour
University of Kentucky (independent)$10n/an/a$40$100
University of Kentucky (assisted)$100$115$345n/an/a
External academic & Non-profit (independent)$75n/an/a$60$150
External academic & Non-profit (assisted)$150$170$520n/an/a
External For-profit (independent)n/an/an/a$80$200
External For-profit (assisted)$200$230$690n/an/a

Independent users are required to use their own microtome/trimmer supplies (knives). Training may be conducted using practice knives (TBD by staff).

For training on instrumentation (microtomes, freezers, small lab equipment), the "Additional staff assistance (Life Sciences sample preparation)" hourly fee will be charged/added to the instrument's independent usage fee.

Sample Preparation Equipment (Life Sciences)

Instrument Name ->Leica CPD300 (per run)Leica EM ICE (per hour)Leica EM AFS2 (per day)Vitrobot (per hour)
Instrument Type ->critical point dryerhigh-pressure freezerfreeze substitutionplunge freezer
University of Kentucky$15$35$35$35
External academic & Non-profit$20$50$50$50
External For-profit$30$70$70$70

Cancellation Policy
48 hours notice must be given to avoid any charges.
Less than 48 hours notice and someone fills your time, there is a two hour charge.
Less than 48 hours notice and no one fills your time, you are charged for your reserved time.

Training
To facilitate training, a fixed number of user hours will be billed at the unassisted rate for each instrument (TBD by EMC), except for Life Sciences sample preparation. Re-training after a long period of user inactivity will be charged at the assisted rate.

After hours and weekends
For after-hours & weekend use by approved, experienced University of Kentucky operators only, the (unassisted) hourly rates for UK internal use will be lowered by 1/3 (33.3%) for electron microscopes, XPS and SAXS. After-hours and weekend access is also possible for non UK users; please contact the EMC staff for details.

External Users
The EMC staff will provide training for external users, and/or provide services by performing the characterization work and, if necessary, specimen preparation. See the pricing chart for external users. In some cases a valid PO number is required before analysis can be scheduled. In such cases it is best to send the PO to the EMC staff directly by email. Typically, external users are not allowed to access the instruments unattended after normal working hours. Normally the information required will be:

  • Purchase order
  • Address where invoice is to be sent
  • Contact person in your business office who will handle this invoice
  • Your own contact information

For industrial users who require confidentiality and intellectual property agreements, please contact the EMC staff directly.

External Users Payment
Payment by check or wire transfer only (no credit card). Payment is due within 30 days of invoicing (Net 30).

1HeliScan microCT operation modes
Two operation modes are available on the HeliScan microCT. The highest resolutions (voxel size) for the tungsten source (W) and the Lanthanum hexaboride (LaB6) sources are ~800 nm and ~400 nm, respectively. The HeliScan microCT is typically configured with the tungsten filament. Switching between sources requires significant equipment re-calibration: access to LaB6 capabilities may be accessible only after a sufficient number of scans are planned by multiple users (TBD by staff).

2Automated sessions
Automated session hours for the electron microscopes, XPS and SAXS (i.e. long unattended runs) are eligible to be billed at a reduced rate: academic/government rate will equal the after-hours rate for that instrument. For-profit business rate is set separately for each instrument, but also includes a reduced rate for automated microCT scans.

3Capped charges for unattended long runs/scans
Available on select instruments (primarily overnight; subject to EMC staff approval and calendar availability). Charges for EM's, XPS, SAXS are capped at 5 hrs (overnight) or 10 hrs (weekend). Charges for microCT are capped at 8 hrs (overnight) or 20 hrs (weekend). Charges for JEOL CCP (cross-section polisher) are capped at 6 hrs, for each individual session.

4Sample preparation equipment
There are separate categories of specimen preparation equipment:

  • Type A: n/a
  • Type B: Leica EM ACE600 carbon & sputter coater will be charged at the rates indicated in the table on a "per run" basis; metallography (low speed precision saw, grinder/polishers, compound microscope, etc.) will be charged on a "per hour" basis. The metallography fee will be waived for the preparation of samples that will be characterized in EMC equipment.